Reacción #2687

Ecuación de reacción

HCl

n-nonadecyl-n-tetradecyl-n-decylcarbinol

calcium chloride

→

n-nonadecyl-n-tetradecyl-n-decylmethylchloride

Disolventes

methylene chloride

Condiciones de reacción

Tratamiento posterior

1. 1
   LavadoThe product mixture is then washed with 1 liter of a 10% sodium carbonate solution
2. 2
   SecadoThe organic layer is dried with magnesium sulfate
3. 3
   Otrothe methylene chloride is evaporated off

Procedimiento

One mole of n-nonadecyl-n-tetradecyl-n-decylcarbinol is added to 0.2 liters of methylene chloride and 0.32 moles calcium chloride. Approximately 1.5 moles of HCl gas is slowly bubbled through the solution. The product mixture is then washed with 1 liter of a 10% sodium carbonate solution. The organic layer is dried with magnesium sulfate and the methylene chloride is evaporated off to give n-nonadecyl-n-tetradecyl-n-decylmethylchloride.

Fuente