Reacción #2507809

Ecuación de reacción

pentacene

maleimide

→

pentacene maleimide

Disolventes

dichlorobenzene

Condiciones de reacción

Tratamiento posterior

1. 1
   TemperaturaThe mixture is cooled to room temperature
2. 2
   Filtraciónthe precipitate is filtered
3. 3
   Lavadowashed with toluene
4. 4
   Otrodried
5. 5
   OtroRecrystallization from dichlorobenzene

Procedimiento

A suspension of pentacene (287 mg, 1 mmole) and maleimide (1 mmole) in 4 mL of dichlorobenzene is heated to 160° C. for 4 hours. The mixture is cooled to room temperature and the precipitate is filtered, washed with toluene and dried. Recrystallization from dichlorobenzene affords pure samples of pentacene-maleimide adduct as white needles.

Fuente