Reacción #2493760

Ecuación de reacción

25

1-(4-(2-(Diethylamino)ethoxy)phenyl)butan-1-amine

1-(4-(2-(pyrrolidin-1-yl)ethoxy)phenyl)butan-1-one

1-(4-(2-(Pyrrolidin-1-yl)ethoxy)phenyl)butan-1-one

→

27

Rendimiento 45.0%

1-(4-(2-(Pyrrolidin-1-yl)ethoxy)phenyl)butan-1-amine

Rendimiento 45.0%

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThe title compound was prepared

Procedimiento

The title compound was prepared by using a similar procedure as described for the preparation of 25 except that 1-(4-(2-(pyrrolidin-1-yl)ethoxy)phenyl)butan-1-one (23) was used instead of 1-(4-(2-(diethylamino)ethoxy)phenyl)butan-1-one (21). This produced crude 27 (188 mg, 45%) as a yellow oil: MS (ES+) m/z 263.2 (M+H)+.

Fuente