Reacción #2383766

Ecuación de reacción

4-chloro-3-methylpyrazole

phosphoric acid

phosphoric acid

→

4chloro-3-methylpyrazolium dihydrogen phosphate

Rendimiento 98.0%

Disolventes

water

Condiciones de reacción

Tratamiento posterior

1. 1
   Otrowas evaporated
2. 2
   workup.WAITAfter a few hours
3. 3
   Otrothe title compound crystallized out of the oil initially present (yield 98%)

Procedimiento

116 g (1.0 mol) of 4-chloro-3-methylpyrazole were dissolved in 115 g (1.0 mol) of phosphoric acid (85%) at room temperature. The water contained in the phosphoric acid was evaporated. After a few hours, the title compound crystallized out of the oil initially present (yield 98%).

Fuente