Reacción #2329048

ord-a2f4640697ca4d7ba20f679bc0875ed9

Ecuación de reacción

Cc1nc2c3cc(Br)ccc3[nH]c(=O)n2n1
9-bromo-2-methyl-6H-[1,2,4]triazolo[1,5-c]quinazolin-5-one
O=c1[nH]c2ccc(Br)cc2c2ncnn12
9-bromo-6H-[1,2,4]triazolo[1,5-c]quinazolin-5-one
Cc1n[nH]c(-c2cc(Br)ccc2N)n1
title compound
Rendimiento 99.0%
Cc1n[nH]c(-c2cc(Br)ccc2N)n1
4-Bromo-2-(5-methyl-2H-[1,2,4]triazol-3-yl)-phenylamine
Rendimiento 99.0%

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

As described for example 23c) 9-bromo-2-methyl-6H-[1,2,4]triazolo[1,5-c]quinazolin-5-one (28.5 g, 102 mmol), instead of 9-bromo-6H-[1,2,4]triazolo[1,5-c]quinazolin-5-one, was converted to the title compound (25.5 g, 99%) which was obtained as an off-white solid. MS: m/e=251.0/253.1 [M−H]−.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07671048B2uspto-grants-2010_03