Reacción #2329036

ord-9bd1e1d60ac142fbbaacce3d10513730

Ecuación de reacción

CCOc1ccc(CCl)cc1
4-ethoxybenzyl chloride
O=S(Cl)Cl
thionyl chloride
CCCCOc1ccc(CO)cc1
4-butoxybenzyl alcohol
CCCCOc1ccc(CCl)cc1
4-Butoxybenzyl Chloride

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    OtroWas synthesized

Procedimiento

Was synthesized following the same general procedure as that for the preparation of 4-ethoxybenzyl chloride; thionyl chloride (7.42 g, 69.2 mmol), 4-butoxybenzyl alcohol (9.45 g, 52.4 mmol), CH2Cl2 (145 mL).

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07671033B2uspto-grants-2010_03