Reacción #2267072

ord-d3e420440800475dbf88c7b2e28ae43e

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    FiltraciónFiltration of the catalyst and evaporation of solvent

Procedimiento

The mixture of compound 10 (3.0 g, 14.3 mmol) and 10% palladium on carbon (1.6 g) in ethanol (230 ml) was stirred under hydrogen for 3 hours. Filtration of the catalyst and evaporation of solvent gave desired product 11 (2.41 g, 94%).

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US06887867B2uspto-grants-2005_05