Reacción #2267055

Ecuación de reacción

pentafluorobenzenesulfonyl chloride

tetramethylammonium hydroxide

→

tetramethylammonium pentafluorobenzenesulfonate

Disolventes

methanol

Condiciones de reacción

Tratamiento posterior

1. 1
   Temperaturacooling

Procedimiento

25 gof pentafluorobenzenesulfonyl chloride was dissolved in 100 ml of methanol under ice-cooling. Then 100 g of a 25% aqueous solution of tetramethylammonium hydroxide was slowly added thereto. By stirring at room temperature for 3 hours, a solution of tetramethylammonium pentafluorobenzenesulfonate was obtained. Thus solution was employed in salt exchange between sulfonium salt and iodonium salt.

Fuente