Reacción #2200579

ord-1c63baaa7b784e589ea1319894e1fcf4

Ecuación de reacción

CCOC(=O)CC(O)CCl
ethyl 4-chloro-3-hydroxybutyrate
C[Si](C)Cl
DMCS
→
CCOC(=O)CC(=O)CCl
Ethyl 4-Chloroacetoacetate

Reactantes

CCOC(=O)CC(O)CCl
ethyl 4-chloro-3-hydroxybutyrate
C[Si](C)Cl
DMCS

Reactivos

Ninguno

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    Otrowas carried out at 150° C

Procedimiento

The quantitation of ethyl 4-chloro-3-hydroxybutyrate was carried out by gas chromatography. Thus, using a glass column (ID 3 mm×1 m) packed with PEG-20M Chromosorb WAW DMCS 10%, 80/100 mesh (product of GL Sciences Inc.), chromatography was carried out at 150° C. The detection was made by FID.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07432095B2uspto-grants-2008_10