Reacción #2195502

Ecuación de reacción

product

9-Benzyl-7,7,11,11-tetrafluoro-1,5-dithia-9-azaspiro[5.5]undecane

→

title compound

1-Benzyl-3,3,5,5-tetrafluoropiperidine

Condiciones de reacción

Tratamiento posterior

1. 1
   Otropurify by silica gel chromatography

Procedimiento

React 4.0 mmol of the product of Example 29 with Raney nickel according to the general procedure set forth in Example 23 and purify by silica gel chromatography using methylene chloride/methanol/saturated NH4OH as eluant to yield the title compound.

Fuente