Reacción #2195501

Ecuación de reacción

product

9-Benzyl-7,7,11,11-tetrafluoro-1,5-dithia-9-azaspiro[5.5]undecane-8,10-dione

lithium aluminum hydride

→

title compound

9-Benzyl-7,7,11,11-tetrafluoro-1,5-dithia-9-azaspiro[5.5]undecane

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroPurify by silica gel chromatography

Procedimiento

React 4.9 mmol of the product of Example 21 with lithium aluminum hydride, using the general procedure set forth in Example 1. Purify by silica gel chromatography using methylene chloride/methanol/saturated NH4OH as eluant to yield the title compound.

Fuente