Reacción #2175510

ord-69ffd4df32b74494be9cc6bdccd1f3d2

Ecuación de reacción

O.O.OC[C@H]1O[C@H](O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@@H](O)[C@@H]1O
trehalose dihydrate
NCC(=O)O
glycine
CC(C[*:1])[*:2]
polypropylene
→
NCC(=O)O.OC[C@H]1O[C@H](O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@@H](O)[C@@H]1O
Trehalose Glycine

Reactantes

O.O.OC[C@H]1O[C@H](O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@@H](O)[C@@H]1O
trehalose dihydrate
NCC(=O)O
glycine
CC(C[*:1])[*:2]
polypropylene

Reactivos

Ninguno

Disolventes

O
water
O
water

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    workup.ADDITIONwas added at room temperature
  2. 2
    Otrowas obtained
  3. 3
    workup.ADDITIONWithout adding any acid

Procedimiento

17.84 g of trehalose dihydrate and 4.03 g of glycine were carefully weighed and transferred into a sterile polypropylene bottle, to which 300 ml of purified water was added at room temperature and stirred slowly until a clear solution was obtained. The pH was measured and found to be 5.5. Without adding any acid, the volume was adjusted to 350 ml with purified water. The pH was measured and found to be 5.5.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US08435943B2uspto-grants-2013_05