Reacción #216907
ord-57fd1430ce8949a6a7d3214a55e2af97
Ecuación de reacción
Quinoline-3-carbaldehyde
L-cysteine
→
2-(3-quinolyl)thiazolidine-4-carboxylic acid
Rendimiento 75.0%
Reactantes
Reactivos
Ninguno
Disolventes
Condiciones de reacción
Condiciones detalladas
See reaction.notes.procedure_details.
Tratamiento posterior
- 1OtroThe resultant crystalline precipitate was collected by suction
- 2Filtraciónfiltrating
- 3Lavadowashed with 50% ethanol
- 4Otrodried
Procedimiento
Quinoline-3-carbaldehyde (1.57 g) and 1.21 g of L-cysteine were dissolved in 50 ml of 50% ethanol, and the solution was stirred at room temperature for 1 hour. The resultant crystalline precipitate was collected by suction filtrating, washed with 50% ethanol and dried to give 1.95 g of 2-(3-quinolyl)thiazolidine-4-carboxylic acid. Melting point 173°-175° C. (decomposition).