Reacción #216833

Ecuación de reacción

diphenyliodonium chloride

lithium tetrakis(pentafluorophenyl)borate

→

diphenyliodonium tetrakis(pentafluorophenyl)borate

Rendimiento 75.0%

Disolventes

water

water

Condiciones de reacción

Tratamiento posterior

1. 1
   TemperaturaThe mixture was maintained
2. 2
   Filtraciónwas then filtered
3. 3
   OtroThe filtrate was dried under reduced pressure (133 Pa) overnight with the exclusion of light
4. 4
   Otro16.33 g (or a yield of 75%) of diphenyliodonium tetrakis(pentafluorophenyl)borate were thus recovered

Procedimiento

7.17 g (or 22.6 mmol) of diphenyliodonium chloride were dissolved in 300 ml of water in a 1,000 ml Erlenmeyer flask. 15.52 g (or 22.6 mmol) of lithium tetrakis(pentafluorophenyl)borate in solution in 250 ml of water were added dropwise. The mixture was maintained under stirring for 30 minutes and was then filtered. The filtrate was dried under reduced pressure (133 Pa) overnight with the exclusion of light. 16.33 g (or a yield of 75%) of diphenyliodonium tetrakis(pentafluorophenyl)borate were thus recovered.

Fuente