Reacción #2146677

ord-17def382435747388118e625c59d519e

Ecuación de reacción

CC1(C)CCCC(C)(C)N1[O]
TEMPO
[Br-].[Na+]
sodium bromide
OO
Hydrogen peroxide
CC1(C)CCCC(C)(C)N1[O].OO
TEMPO H2O2

Reactivos

Ninguno

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    workup.ADDITIONA sample of cotton textile (ca. 1 g) is added to a solution
  2. 2
    LavadoThe material is washed with water
  3. 3
    Otrodried

Procedimiento

A sample of cotton textile (ca. 1 g) is added to a solution composed of 90 mL water with 10 mg (0.065 mmol) TEMPO and 0.22 g (2 mmol) sodium bromide. Hydrogen peroxide 3% is added (0.9 mL, 1 mmol) and the reaction stirred at RT for 10 minutes to 2 hours. The material is washed with water, dried, and used without further modification in the following ZnO deposition step.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US08277518B1uspto-grants-2012_10