Reacción #2076844

ord-13814129c9fe4366b1e883b3c4bbebc4

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

The title compound was prepared from 6′-bromo-6-methyl-4-(4-trifluoromethylphenyl)-[2,2′]bipyridinyl (example E.26) (0.39 g, 1.1 mmol) and commercially available (3-methylsulfonylphenyl)boronic acid (0.218 g, 1.0 mmol) according to the general procedure VI. Obtained as a white solid (0.420 g, 90%). MS (ISP) 469.1 [(M+H)+]; mp 186° C.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07642264B2uspto-grants-2010_01