Reacción #2075714

ord-9a9f0a1470984ce2842aab81852b12a4

Ecuación de reacción

ClOCl.[Zr]
zirconium oxychloride
O=S(=O)([O-])[O-].[Na+].[Na+]
sodium sulfate
Cl
hydrochloric acid
O=S(=O)([O-])[O-].O=S(=O)([O-])[O-].[Zr+4]
zirconium sulfate

Condiciones de reacción

Temperatura
75°CELSIUS
Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    Temperaturamaintained for 1 hour to age

Procedimiento

625 g of a 16% (ZrO2 conversion) zirconium oxychloride solution at room temperature was added to 237 g of a 25% sodium sulfate solution. After addition of hydrochloric acid to achieve a free acid concentration of 1.5 N, this was heated to 75° C. and maintained for 1 hour to age while producing basic zirconium sulfate.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07642210B2uspto-grants-2010_01