Reacción #2021473

Ecuación de reacción

perfluorooctanesulfonic acid

silver carbonate

→

silver perfluorooctanesulfonate

Disolventes

water

Condiciones de reacción

Tratamiento posterior

1. 1
   workup.ADDITIONwas added
2. 2
   workup.STIRRINGAfter stirring at room temperature for 3 days
3. 3
   Filtraciónthe mixture was filtered
4. 4
   Filtraciónthe obtained filter-cake
5. 5
   Lavadowas washed with 10 parts of ion-exchange water
6. 6
   Secado20 parts of diethylether and dried

Procedimiento

Into a four-necked flask were charged 75 parts of perfluorooctanesulfonic acid and 100 parts of water, and 21.4 parts of silver carbonate was added thereto with stirring. After stirring at room temperature for 3 days, the mixture was filtered and the obtained filter-cake was washed with 10 parts of ion-exchange water, then 20 parts of diethylether and dried to give 60.3 parts of silver perfluorooctanesulfonate.

Fuente