Reacción #1973963

Ecuación de reacción

3,4-dinitroaniline

methanesulfonyl chloride

pyridine

→

title compound

N-(3,4-dinitrophenyl)methanesulfonamide

Disolventes

CH2Cl2

Condiciones de reacción

Tratamiento posterior

1. 1
   ConcentraciónMixture was concentrated under vacuum

Procedimiento

A mixture of 3,4-dinitroaniline (5.27 g, 28.8 mmol), methanesulfonyl chloride (3.36 mL, 43.1 mmol) and pyridine (5.82 mL, 71.9 mmol) in CH2Cl2 (100 mL) was stirred for 24 h. Mixture was concentrated under vacuum to provide a crude semi-solid title compound that was used without further purification.

Fuente