Reacción #1960480

ord-118de9a10e8743beb8e2aa4830d270e5

Ecuación de reacción

CCCCCCCCCCCCCCCCCC(=O)O
stearic acid
[Na+].[OH-]
sodium hydroxide
O=[N+]([O-])[O-].[Ag+]
silver nitrate
CCCCCCCCCCCCCCCCCC(=O)[O-].[Ag+]
silver stearate

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    workup.DISSOLUTIONwere completely dissolved
  2. 2
    workup.STIRRINGthe result was stirred for 3 hours
  3. 3
    OtroWhite powder on the surface of the result was collected
  4. 4
    Lavadowashed three times each with distilled water

Procedimiento

7.5 g of stearic acid and 1.2 g of sodium hydroxide were added to 300 ml of water and sufficiently stirred until they were completely dissolved. 5.2 g of silver nitrate was added thereto, and the result was stirred for 3 hours. White powder on the surface of the result was collected and washed three times each with distilled water and with methanol to obtain silver stearate. An anode active material was prepared as in Example 1, except that silver stearate was used instead of nickel stearate, the molar ratio of silver to silicon was 0.2:1, the weight ratio of silicon to graphite was 0.5:1, and the carbon layer was 5.2 wt % of the anode active material.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: USRE043794E1uspto-grants-2012_11