Reacción #1946553

ord-4c0b174462974ac89e2b7c1c36a908e1

Ecuación de reacción

CCCCCCCCCCCC(=O)N(C)CC(=O)O
N-lauroylsarcosine
O=S(=O)(O)O
sulfuric acid
→
CCCCCCCCCCCC(=O)N(C)CC(=O)OCCCC
N-lauroylsarcosine butyl ester

Reactantes

CCCCCCCCCCCC(=O)N(C)CC(=O)O
N-lauroylsarcosine
O=S(=O)(O)O
sulfuric acid

Reactivos

Ninguno

Disolventes

CCCCO
1-butanol

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    TemperaturaThe mixture was heated
  2. 2
    Temperaturaunder reflux for reaction for 6 hours

Procedimiento

One hundred and thirty-five point five(135.5) grams of N-lauroylsarcosine (ex. Kawaken Fine Chemicals Co., Ltd.) and 200 ml of 1-butanol were charged into a 500-milliliter flask. Further, 4.99 g of conc. sulfuric acid were added as the catalyst. The mixture was heated under reflux for reaction for 6 hours.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US06528068B1uspto-grants-2003_03