Reacción #1946550

ord-8bcbfa809426476db72b76e486fe6dd5

Ecuación de reacción

CCCCCCCC(=O)N(C)CCC(=O)O
N-octanoyl-N-methyl-β-alanine
CC(C)O
isopropanol
O=S(=O)(O)O
sulfuric acid
→
CCCCCCCC(=O)N(C)CCC(=O)OC(C)C
N-octanoyl-N-methyl-β-alanine isopropyl ester

Reactantes

CCCCCCCC(=O)N(C)CCC(=O)O
N-octanoyl-N-methyl-β-alanine
CC(C)O
isopropanol
O=S(=O)(O)O
sulfuric acid

Reactivos

Ninguno

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    TemperaturaThe mixture was heated
  2. 2
    Temperaturaunder reflux
  3. 3
    Otroreaction for 8 hours

Procedimiento

Fifty-seven(57) grams of N-octanoyl-N-methyl-β-alanine and 500 ml of isopropanol were charged into a 1,000-milliliter flask, and 1 ml of conc. sulfuric acid was further added thereto as the catalyst. The mixture was heated under reflux reaction for 8 hours.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US06528068B1uspto-grants-2003_03