Reacción #1921526

Ecuación de reacción

p-toluenesulfonic-acid-(2-ethoxyethyl)-ester

2,3,6-trimethylaniline

→

N-(2-ethoxyethyl)-2,3,6-trimethyl-aniline

Rendimiento 68.0%

Disolventes

toluene

Condiciones de reacción

Procedimiento

According to the method of Example 1a 553 g (2.26 moles) of p-toluenesulfonic-acid-(2-ethoxyethyl)-ester are added to a solution of 607 g (4.5 moles) 2,3,6-trimethylaniline in 1 liter of toluene. 317 g(68% of theoretical amount) of N-(2-ethoxyethyl)-2,3,6-trimethyl-aniline are obtained, b.p. 150°-152° C / 14 Torr.

Fuente