Reacción #1904060

ord-1c00fd48005142318f15caba8be7b47a

Ecuación de reacción

CC(C)(O)c1cc(Br)ccc1N
2-(2-amino-5-bromophenyl)propan-2-ol
O=C(Cl)CCl
chloro acetyl chloride
CC(C)(O)c1cc(Br)ccc1NC(=O)CCl
N-[4-Bromo-2-(1-hydroxy-1-methyl-ethyl)-phenyl]-2-chloro-acetamide

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

Prepared from 2-(2-amino-5-bromophenyl)propan-2-ol and chloro acetyl chloride generally according to the procedure described in example 1. An off-white solid: mp 133-134° C. 1H-NMR (DMSO-d6) δ 11.21 (s, 1H), 8.12 (d, J=8.6 Hz, 1H), 7.46 (dd, J=8.6, 2.3 Hz, 1H), 7.44 (d, J=2.3 Hz, 1H), 6.28 (s, 1H), 4.43 (s, 2H), 1.53 (s, 6H).

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07598237B2uspto-grants-2009_10