Reacción #1904041
ord-5e11c941b17046ef94b03835ee80a6cd
Ecuación de reacción
p-bromophenol
benzyl bromide
→
4-benzyloxybromobenzene
Reactivos
Ninguno
Disolventes
Condiciones de reacción
Temperatura
80°CELSIUS
Condiciones detalladas
See reaction.notes.procedure_details.
Tratamiento posterior
- 1workup.ADDITIONwere added
Procedimiento
To a solution composed of p-bromophenol (17.3 g, 0.1 mol) and dry DMF (100 mL), anhydride K2CO3 (8.28 g, 0.06 mmol) and benzyl bromide (25.6 g, 0.15 mmol) were added. The mixture was stirred at 80° C. under a nitrogen atmosphere for six hours. Then, the reaction mixture was charged into 500 mL of ice water.