Reacción #1885010
ord-84a817739218448f800ce098b60147f5
Ecuación de reacción
styrene
butyl acrylate
acrylic acid
dodecanethiol
sodium dodecylbenzenesulfonate
→
Styrene Butyl Acrylate Acrylic Acid
Reactivos
Ninguno
Disolventes
Condiciones de reacción
Condiciones detalladas
See reaction.notes.procedure_details.
Tratamiento posterior
- 1OtroIn a reactor equipped with a reflux condenser, a stirrer
- 2workup.ADDITIONa nitrogen-introducing pipe
Procedimiento
In a reactor equipped with a reflux condenser, a stirrer, a nitrogen-introducing pipe, and a monomer dripping funnel, 3.3 parts of sodium dodecylbenzenesulfonate is dissolved in 3,824 parts of ion exchange water. Subsequently, 30.6 parts of styrene, 9.4 parts of butyl acrylate, 1.2 parts of acrylic acid dimer, and 0.3 parts of dodecanethiol are added thereto, and thoroughly stirred at room temperature for emulsification stabilization (emulsified liquid 1).