Reacción #1880949

ord-e3da1ad9914a4f978033cb83e4daf5c9

Ecuación de reacción

OCCC1CCCCC1
Cyclohexylethyl alcohol
C=COCC
ethyl vinyl ether
C=COCCC1CCCCC1
cyclohexylethyl vinyl ether

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    OtroThe resultant reaction mixture
  2. 2
    Extracciónwas extracted with ethyl acetate and water
  3. 3
    Lavadothe extract was washed with water
  4. 4
    workup.DISTILLATIONdistilled under reduced pressure

Procedimiento

Cyclohexylethyl alcohol was mixed with ethyl vinyl ether. Mercury acetate was added thereto and this mixture was stirred at room temperature for 12 hours. The resultant reaction mixture was extracted with ethyl acetate and water, and the extract was washed with water and then distilled under reduced pressure to obtain cyclohexylethyl vinyl ether (X-1) as the target compound.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07022456B2uspto-grants-2006_04