Reacción #1876821
ord-a9e2bc7ece64422aa680ac0d6978bd7c
Ecuación de reacción
1,3-dichloroformyl-5-hydroxyadamantane
trimethylamine
trimethylsilyl chloride
→
1,3-dichloroformyl-5-trimethylsiloxyadamantane
Reactivos
Ninguno
Disolventes
Condiciones de reacción
Condiciones detalladas
See reaction.notes.procedure_details.
Tratamiento posterior
- 1OtroReaction
- 2Otrowas carried out at room temperature
Procedimiento
The 1,3-dichloroformyl-5-hydroxyadamantane was dissolved in methylene chloride. To this solution were added a small amount of trimethylamine, and then an eguimolar amount of trimethylsilyl chloride. Reaction was carried out at room temperature to obtain 1,3-dichloroformyl-5-trimethylsiloxyadamantane.