Reacción #1869202

ord-60614bbfc0554c2f9387e571239d1365

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    Otrothe reaction mixture was evaporated to dryness

Procedimiento

1,1-dimethylethyl {1-[2-(4-quinolinyl)ethyl]-4-piperidinyl}carbamate (9a) (278 mg) was dissolved in chloroform and diluted with 4N HCl in dioxane solution. After stirring two hours, the reaction mixture was evaporated to dryness to afford the product as a solid (180 mg, 100%).

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07498326B2uspto-grants-2009_03