Reacción #1860

ord-d735999e237040e79efd9e34aa9e36bf

Ecuación de reacción

CCOC(=O)CBr
ethyl bromoacetate
CSC
dimethyl sulfide
CCOC(=O)C[S+](C)C.[Br-]
title compound
CCOC(=O)C[S+](C)C.[Br-]
Carboethoxymethyl Dimethylsulfonium Bromide

Reactivos

Ninguno

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

A solution of ethyl bromoacetate (265 g) and dimethyl sulfide (114 g) in acetone (500 mL) was stirred at room temperature. After three days, the title compound was isolated by filtration of the reaction mixture. Melting point 88°-90° C.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US05726320uspto-grants-1998_03