Reacción #1839

ord-61857a4aa4ad49af8aac9e9223a18f71

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    Otroafter purification over silica gel with n-heptane/ethyl acetate (3:2), 10.3 g of oily crude product

Procedimiento

10 g (60 mmol) of 5-hydroxy-2-nitrobenzyl alcohol were reacted with 7.0 ml (70 mmol) of isopropyl iodide analogously to Example 4a); after purification over silica gel with n-heptane/ethyl acetate (3:2), 10.3 g of oily crude product.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US05726305uspto-grants-1998_03