Reacción #1732

Ecuación de reacción

alkyne

2-(hex-1-ynyl)-9,9-dimethyl-6,7,8, 9-tetrahydro-5H-benzocycloheptene

→

2-hexyl-9,9-dimethyl-6,7,8,9-tetrahydro-5H-benzocycloheptene

Disolventes

ethy acetate

Condiciones de reacción

Tratamiento posterior

1. 1
   FiltraciónFiltration
2. 2
   Otroover diatomaceous earth and removal of the solvent

Procedimiento

This alkyne was dissolved in 30 ml of ethy acetate and hydrogenated over 2 g of Pd/C (10%) at room temperature and under 1 atm H2. Filtration over diatomaceous earth and removal of the solvent gave 3.08 g of 2-hexyl-9,9-dimethyl-6,7,8,9-tetrahydro-5H-benzocycloheptene as a colorless oil (GC purity: 98%).

Fuente