Reacción #1730514

ord-a99cdb66714644ba8381f1cfe23b712b

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    OtroMethanol is removed by fractionated distillation
  2. 2
    OtroThe resulting aqueous solution is used as an emulsifier in the polymerization of fluorinated olefins

Procedimiento

The calculated yield was 59% based on total PPVE used; 70% based on converted PPVE. The ester is converted to the ammonium salt by reaction with aqueous ammonia. Methanol is removed by fractionated distillation. The resulting aqueous solution is used as an emulsifier in the polymerization of fluorinated olefins.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US08119750B2uspto-grants-2012_02