Reacción #1700441

Ecuación de reacción

n-butanol

δ-n-butyl o-phenoxybenzyl cyanide

sulfuric acid

→

product

Rendimiento 104.9%

n-Butyl-2-(o-phenoxyphenyl)hexanoate

Rendimiento 104.9%

Disolventes

water

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroInto a 500-ml round bottom flask are placed
2. 2
   TemperaturaThe mixture is heated
3. 3
   Temperaturato reflux overnight
4. 4
   TemperaturaIt is then cooled
5. 5
   Extracciónextracted with toluene
6. 6
   LavadoThe combined extracts are washed with water
7. 7
   Secadodried over MgSO4
8. 8
   OtroSolvent is evaporated

Procedimiento

Into a 500-ml round bottom flask are placed 77.7 g (1 mole) of n-butanol, 36.5 g (0.14 mole) of δ-n-butyl o-phenoxybenzyl cyanide and 14.4 g (0.45 mole) of conc. sulfuric acid. The mixture is heated to reflux overnight. It is then cooled, poured into water and extracted with toluene. The combined extracts are washed with water and dried over MgSO4. Solvent is evaporated to give 50 g of product.

Fuente