Reacción #1687647

Ecuación de reacción

( 3 )

4-acetoxy-2-fluoro-1-(1-ethylpropyloxycarbonyl)benzene

benzylamine

→

4-hydroxy-2-fluoro-1-(1-ethylpropyloxycarbonyl)benzene

Disolventes

ether

ethanol

Condiciones de reacción

Tratamiento posterior

1. 1
   Lavadothe diluted mixture was washed with diluted hydrochloric acid
2. 2
   Secadowith water and dried over magnesium sulfate

Procedimiento

0.5 Gram of the compound obtained in the above (3) was dissolved in 30 ml of ethanol, and 1.5 g of benzylamine was added dropwise thereto. Further, the mixture was stirred at room temperature for one day and diluted with 300 ml of ether, and the diluted mixture was washed with diluted hydrochloric acid and then with water and dried over magnesium sulfate.

Fuente