Reacción #1631

Ecuación de reacción

cyclohexylphosphinic acid, n-butyl ester

paraformaldehyde

→

title compound

Cyclohexylhydroxymethylphosphinic acid, n-butyl ester

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroPurification by chromatography
2. 2
   Lavadoeluting with dichloromethane containing 5% methanol
3. 3
   Otrogave an oil

Procedimiento

The title compound was prepared from cyclohexylphosphinic acid, n-butyl ester and paraformaldehyde according to the method described in Procedure 31. Purification by chromatography, eluting with dichloromethane containing 5% methanol, gave an oil.

Fuente