Reacción #1618422

Ecuación de reacción

3,5-dibromo-2-hydroxybenzaldehyde

N-tert-butylhydroxylamine

→

title compound

α-(3,5-Dibromo-2-hydroxyphenyl)-N-tert-butylnitrone

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThe title compound was prepared

Procedimiento

The title compound was prepared according to the procedure described in Example 13 using 3,5-dibromo-2-hydroxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 68.7% yield as a yellow crystalline solid, m.p. 111.3° C. (Rf=0.54 on a silica gel plate using 7:3 hexanes/EtOAc as an eluant).

Fuente