Reacción #159282

ord-3e84eb0ed57b475cbbdee34bf3c5aaeb

Reactivos

Ninguno

Condiciones de reacción

Temperatura
100°CELSIUS
Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    OtroExcess butyric anhydride was then removed under reduced pressure
  2. 2
    Otroto provide a solid residue that
  3. 3
    Otrowas recrystallized from ethanol

Procedimiento

5 g of phenylalanine was added to 20 mL of butyric anhydride and the resulting mixture heated to about 100° C. for about 3 h. Excess butyric anhydride was then removed under reduced pressure to provide a solid residue that was recrystallized from ethanol to provide phenylalanine butyramide.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US08828960B2uspto-grants-2014_09