Reacción #157904

ord-81dc4ea8c152498aaf44befe36b0dc78

Reactivos

Ninguno

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    Otrois in the temperature range of about 85° C. to about 95° C
  2. 2
    Otroto form a dark slurry
  3. 3
    Otroresulted
  4. 4
    FiltraciónThe product was filtered in a Büchner funnel
  5. 5
    Lavadothe cake was washed with deionized water
  6. 6
    Otrodrying

Procedimiento

200 g of disodium tetraborate was dissolved in 800 ml of hot deionized water. The water is in the temperature range of about 85° C. to about 95° C. 150 g of 45% titanium III sulfate was added to the above solution to form a dark slurry. 35% H2O2 was added drop-wise to the slurry until a homogenous yellow suspension resulted. The product was filtered in a Büchner funnel, and the cake was washed with deionized water. Solids were determined to be 19.8% by oven drying.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US08822582B2uspto-grants-2014_09