Reacción #1515623

ord-1c887ca10d8a463fb28cd1f5ba0676b9

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    workup.ADDITIONThe resultant was treated in the same manner

Procedimiento

1-methylnaphthalene (142 mg), methacryloyl chloride (110 mg), and aluminium chloride (160 mg) were reacted in dichloromethane (1.5 mL) at from −30° C. to room temperature for 4 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (122 mg).

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US08937091B2uspto-grants-2015_01