Reacción #1512821

ord-037de5ec15f449a482da554209bd3db4

Ecuación de reacción

CN1c2ccccc2C(C(=O)O)c2ccccc21
10-methylacridan-9-carboxylic acid
CN1c2ccccc2C(C(=O)O)c2ccccc21
10-Methylacridan-9-carboxylic acid
O=S(Cl)Cl
thionyl chloride
→
CN1c2ccccc2C(C(=O)Cl)c2ccccc21
10-Methylacridan-9-carboxylic acid chloride

Reactantes

CN1c2ccccc2C(C(=O)O)c2ccccc21
10-methylacridan-9-carboxylic acid
CN1c2ccccc2C(C(=O)O)c2ccccc21
10-Methylacridan-9-carboxylic acid
O=S(Cl)Cl
thionyl chloride

Reactivos

Ninguno

Disolventes

ClCCl
dichloromethane

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

A solution of 0.35 parts of 10-methylacridan-9-carboxylic acid (77) in 20 mL dichloromethane and 1.1 parts of thionyl chloride is treated as described in Example I, to give 10-Methylacridan-9-carboxylic acid chloride.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US08932881B2uspto-grants-2015_01