Reacción #1495471

ord-01f40b83c3e945a188fde6a54faa81a4

Reactivos

Ninguno

Condiciones de reacción

Temperatura
130°CELSIUS
Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    OtroA four-necked rounded bottom flask equipped with a stirrer
  2. 2
    Otroan esterification reaction
  3. 3
    OtroA reaction product was purified with methyl ether

Procedimiento

A four-necked rounded bottom flask equipped with a stirrer, a thermocouple, and a nitrogen inlet tube was charged with 1 mol of behenic acid per mol of behenyl alcohol, and the contents were heated to 130° C. for 3 hours in a nitrogen atmosphere to carry out an esterification reaction. A reaction product was purified with methyl ether to provide behenyl behenate. Here, the acid value was 0.1 mgKOH/g, and the hydroxyl value was 1.2 mgKOH/g

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US08921022B2uspto-grants-2014_12