Reacción #1464564

Ecuación de reacción

2-methylbenzoxazole

n-octyl iodide

→

3-n-octyl-2-methylbenzoxazolium iodide

Rendimiento 73.2%

Disolventes

ether

Condiciones de reacción

Tratamiento posterior

1. 1
   Temperaturaat reflux for 18 h
2. 2
   TemperaturaAfter cooling
3. 3
   Filtraciónfiltered
4. 4
   Lavadowashed with ether
5. 5
   Otrodried

Procedimiento

A stirred solution of 2-methylbenzoxazole (10.0 g, 75 mmol) and n-octyl iodide (18.0 g, 75 mmol) was heated at reflux for 18 h. After cooling, the yellow-brown solid was slurried in ether, filtered and washed with ether. The resulting solid was air dried to give (20.5 g, 73%) of 3-n-octyl-2-methylbenzoxazolium iodide.

Fuente