Reacción #1464563

Ecuación de reacción

2-methylbenzoxazole

n-pentyl iodide

→

3-n-pentyl-2-methylbenzoxazolium iodide

Rendimiento 82.0%

Disolventes

ether

Condiciones de reacción

Tratamiento posterior

1. 1
   Temperaturaat reflux for 18 h
2. 2
   TemperaturaAfter cooling
3. 3
   Filtraciónfiltered off
4. 4
   Lavadowashed with ether
5. 5
   Otrodried

Procedimiento

A stirred solution of 2-methylbenzoxazole (10 g, 75 mmol) and n-pentyl iodide (14.85 g, 75 mmol) was heated at reflux for 18 h. After cooling, the yellow-brown solid was slurried in ether, filtered off and washed with ether. The resulting solid was air dried to give 3-n-pentyl-2-methylbenzoxazolium iodide (20.3 g, 82%).

Fuente