Reacción #1447094

Ecuación de reacción

Acetic anhydride

4-bromo-3-methoxy-phenylamine

→

N-(4-Bromo-3-methoxy-phenyl)-acetamide

Disolventes

acetic acid

—

ice

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThe precipitate is separated by filtration
2. 2
   Lavadowashed with water
3. 3
   Otrodried at 60° C.
4. 4
   Otroto give the product

Procedimiento

Acetic anhydride (13 mL) is added to an ice-cold solution of 4-bromo-3-methoxy-phenylamine (25.0 g) in acetic acid (100 mL). The mixture is stirred for 1 h and then diluted with ice-cold water (500 mL). The precipitate is separated by filtration, washed with water and dried at 60° C. to give the product.

Fuente