Reacción #1375339
ord-0f4689fa441b486e8cf37d29ba3a9042
Ecuación de reacción
Reactivos
Ninguno
Condiciones de reacción
Condiciones detalladas
See reaction.notes.procedure_details.
Procedimiento
1,2,4,5-Tetrahydro-8,11-dimethyl-3H-azepino[4,5-b]quinoline, 2,3,4,5-tetrahydro-8,11-dimethyl-1H-azepino[4,5-b]quinoline and their dihydrochlorides were prepared from hexahydro-azepinone-(4) hydrochloride and 2-amino-4-methyl-acetophenone analogous to Example 127. Yield of the dihydrochloride of the [4,5-b]-isomer: 17% of theory; m.p. 290°-292° C. (decomp.).