Reacción #1371569

ord-b2262c1e853e40f5b238d09468e2e392

Ecuación de reacción

COC(=O)C(C)c1ccc2cc(O)ccc2c1
methyl 6-hydroxy-2-naphthyl-α-methylacetate
COCCl
chlorodimethyl ether
COCOc1ccc2cc(C(C)C(=O)OC)ccc2c1
methyl 6-methoxymethyloxy-2-naphthyl-α-methylacetate

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    workup.ADDITIONA mixture of 23 g
  2. 2
    OtroThe reaction mixture is evaporated under reduced pressure

Procedimiento

A mixture of 23 g. of methyl 6-hydroxy-2-naphthyl-α-methylacetate, 25 g. of chlorodimethyl ether, and 500 ml. of dimethylformamide is allowed to stand at room temperature for 12 hours. The reaction mixture is evaporated under reduced pressure to give methyl 6-methoxymethyloxy-2-naphthyl-α-methylacetate.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US03978124uspto-grants-1976_08