Reacción #1369

ord-141b4f862c4146f6950ca566cd749152

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    Temperaturathe mixture is refluxed for 1 hour
  2. 2
    ConcentraciónAfter concentrating

Procedimiento

To 2-methyl-3,4,6-trifluorobenzoic acid (3.2 g) is added thiony chloride (7 ml) and the mixture is refluxed for 1 hour. After concentrating, 2-methyl-3,4,6-trifluorobenzoyl chloride (3.3 g) is obtained.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US05723648uspto-grants-1998_03