Reacción #1365706

ord-8df9a23df07745eab43ba41bd6dfb9e9

Ecuación de reacción

COc1ccc(C=O)cc1
Anisaldehyde
CC(=O)O
acetic acid
O=S(=O)(O)O
sulfuric acid
→
COc1ccc(C=O)cc1.O=S(=O)(O)O
Anisaldehyde sulfuric acid

Reactantes

COc1ccc(C=O)cc1
Anisaldehyde
CC(=O)O
acetic acid
O=S(=O)(O)O
sulfuric acid

Reactivos

Ninguno

Disolventes

CO
methanol

Condiciones de reacción

Temperatura
100°CELSIUS
Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

Anisaldehyde (0.5 ml) is mixed with glacial acetic acid (10 ml), methanol (85 ml) and concentrated sulfuric acid (5 ml). This solution is sprayed onto the TLC plate, which is then heated at 100° C.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US06444233B1uspto-grants-2002_09