Reacción #1355839

ord-7dd2c8bd187d477f979ec8c0ccba6bef

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

Example 11 describes the procedure for producing 1,3-bis(ferrocenylethynyl)benzene 516. Ethynylferrocene 500 was reacted with 1,3-diiodobenzene 502 to form 1-(ferrocenylethynyl)-3-iodobenzene 504. Sufficient ethynylferrocene 500 was present such that the second step of the reaction immediately proceeded. 1-(Ferrocenylethynyl)-3-iodobenzene 504 reacted with ethynylferrocene 514 to form 1,3-bis(ferrocenylethynyl)benzene 516. The reaction procedure is shown in FIG. 5.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07198771B2uspto-grants-2007_04